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Definition
Ray - path of the light wave
Cone of light is focused by a lens on the object |
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Definition
the angle of incidence equals the angle of reflection |
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Ibn Sahl
Wellebrord Snellius |
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Law of Refraction
n1 sin(theta1) = n2 sin(theta2) |
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Definition
Huygens principle states that a wavefront can be thought of as an infinite number of hemispherical wavefronts
allowed scientists to understand particle-wave duality of light |
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Definition
invented after 1600
followed the invention of the telescope in 1608
no reliable date of invention, given to prominent people
Hans Maartens |
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Definition
Developed the early electron microscope
Invented osciolloscope to prevent power surges
used oscilloscope to create the electron microscope |
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Definition
equation for resolution
cannot see details smaller than wavelength of light
detail resolved in sample is about half the wavelength at best |
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Definition
the point at which light (parallel rays) converges after passing through a biconvex lens
fixed in light microscopes
variable in electromagnetic microscopes |
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Definition
where the object is placed (where the rays are parallel) (-u) |
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Definition
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Definition
the distance to the focal point (in the back space) (+v) |
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Definition
ray tracing: rays arriving on axis go parallel to their direction in the front space
all other rays are refracted, converged in biconvex lens |
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Definition
1/v-1/(-u)=1/f becomes 1/v+1/u=1/f
M (magnification) = v/u
if u=v=2f, then M = 1x |
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Term
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Definition
1. In SEM, the lenses only exist to focus the beam from the source
2. resolution depends on spot size. you don't want to magnify the image of the source very much
3. magnification relationship not too far from reality
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Term
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Definition
showed that a flowing current generates a magnetic field (lead to electromagnetic lens) |
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Term
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Definition
spiral turn of wire, at the heart of the electromagnetic lens |
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Term
geometric optics in electrons |
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Definition
1. electron spirals through the lens
2. no change in velocity as in the light lens
3. same lens equations hold true |
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Term
Difference between SEM and TEM |
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Definition
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Term
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Definition
the distance of the object from the objective lens |
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Term
depth of field vs working distance |
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Definition
shorter working distance = smaller depth of field |
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Term
Major difference between light and electrons |
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Definition
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Term
voltage vs wavelength of electron |
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Definition
higher voltage = shorter wavelength |
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Term
basic equation for resolution |
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Definition
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Term
equation for numerical aperture |
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Definition
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Term
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Definition
the smallest distance between details you can see in the image |
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Term
does NA remain the same regardless of where one is in the raster pattern? |
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Definition
No, changes with the raster pattern |
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Term
how does aperture effect gathering power and resolution? |
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Definition
large spot = better gathering power, low resolution
small spot = poor gathering power, high resolution |
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Term
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Definition
occurs whenever waves interact with matter
huygens' principle |
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Term
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Definition
lowest in polepiece lens
intermediate in shrouded lens
greatest in simple solenoid |
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Term
Why is the polepiece lens used? |
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Definition
electrons spent too much time in lens
coated lens in iron with brass piece
entire field emitted through brass piece, making smaller, thinner lens (better)
condensed electron field thin as pancake, close to ideal lens |
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Term
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Definition
rays far from axis converge close to the lens
rays near axis converge further from lens
creates a circle of minimum confusion instead of a focal point |
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Term
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Definition
different wavelengths of light converge differently
blue focuses closer, red is further away
opposite in electron microscope |
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Term
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Definition
rays converge asymmetrically, refraction stronger in one direction than another |
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Term
how is astigmatism caused in electron microcopes? |
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Definition
volatiles from sample and oils from pump insulate parts of the lens and magnetic field |
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Term
how is astigmatism corrected in electron microcopes? |
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Definition
stigmator
charged poles pull the beam on one direction or another, can change the direction and magnitude of the pull |
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Term
airy's disk with interference fringes |
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Definition
d = contains half the beam current |
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Term
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Definition
elastic - bouncing off protons
inelastic - knocks electrons out of electron shell |
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Term
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Definition
IR, visible, UV
fluorescence
electron orbitals |
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Term
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Definition
differ in terms of energy
n = quantum number of electron shell
increasing energy with increasing n
E = nhf |
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Definition
incoming electron knocks out electron from an atom, electron fills from another quantum shell, releasing x-radiation |
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Term
Bohr theory of atomic structure |
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Definition
electrons move around nucleus in energy levels
more energy at higher levels
equation for angular momentum
explains frequency of hydrogen irradiance spectrum
n=/=0
couldn't solve anything other than hydrogen |
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Term
Pauli exclusion principle |
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Definition
No 2 electron orbitals can have the same quantum signature
azimuthal, spin |
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Term
Heisenberg uncertainty principle |
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Definition
cannot measure the state of 2 electrons (one disturbs the other) |
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Term
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Definition
increasing voltage increases interactions (zone of interaction)
low voltage = minimal elastic and inelastic scattering |
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Term
energy of emitted electrons |
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Definition
determined by atomic structure |
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Term
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Definition
how far the electron moves without colliding (elastic)
shorter for larger atoms, reason for coating |
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Term
Peak III (from e- emission graph) |
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Definition
secondary electrons, kept from inventing a usable electron microscope |
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Term
how are electrons captured? |
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Definition
positive field
electrons are "lazy" and change trajectory easily
boost +10kV before scintillator, to keep from getting stuck
scintillator made of scintillin produces photons when electrons strike |
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Term
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Definition
made of scintillin
beta emmitter
converts electrons into photons
some electrons lost on the sides of the scintillator |
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Term
describe the path of the signal through the secondary signal detector? |
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Definition
collimator and high voltage lead (aluminum) attracts electrons > scintillator (electrons>photons) > light pipe (quartz or lucite) > photocathode (converts photons>photoelectrons) > photomultiplier tube (PMT; amplifies photoelectrons into a usable signal, gain increased at each dynode) > CRT |
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Term
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Definition
after light tube, converts photons from scintillator into photoelectrons |
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Term
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Definition
photomultiplier tube
amplifies the signal at each dynode and sends it to the CRT |
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Term
Everhart Thornley Detector |
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Definition
The most common design for a secondary detector |
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Term
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Definition
usually doughnut shape under the final lens, can be in the same port as the secondary detector |
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Term
Why two different detectors? (graph) |
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Definition
Two different types of scattering
Emission energy as a fraction of beam energy
Region I. backscatter, Region II. backscatter with energy loss, Region III. secondary emission |
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Term
backscatter efficiency vs atomic number |
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Definition
high atomic number means high backscatter |
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Term
mean path property (mean free path) |
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Definition
electron beam will go deep into sample with low density and atomic weight
can go a long distance without colliding |
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Term
z contrast (atomic number contrast) |
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Definition
if z is high then high brighness |
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Term
signal noise relationship in the secondary detector |
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Definition
signal bounces off specimen (100 electrons)
scintillator boosts signal strength
60-70 quanta per 100 quanta |
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