Shared Flashcard Set

Details

Pressure review
Review of lab pressure concepts
21
Chemistry
Undergraduate 4
12/07/2014

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Cards

Term
What are the types of pumps?
Definition
1]mechanical pump
2]turbomolecular pump
3]diffusion pump
4]ion pump
5]sublimation pump
6]cryo pump
Term
What are the pressure regions and associated pressure range?
Definition
Region A [760 to 10^-4 Torr]
Region B [10^-4 to10^-8 Torr]
Region C [10^-8 to 10^-11 Torr]
Region D [10^-11 to 10^-15 Torr]
Term
What pump(s) are required to reach Region A (760 to 10^-4 Torr)?
Definition
Mechanical pump (Roughing pump)
Term
What pump(s) are required to reach region B [10^-4 to10^-8 Torr]
Definition
Combination of heat and mechanical pump in addition to either a turbo pump or diffusion pump.
Term
What pump(s) are required to reach region C [10^-8 to 10^-11 Torr]?
Definition
Requires heating to 200C+ in addition to a mechanical pump plus a turbo or diffusion pump and an ion, sublimation or cryo pump.
Term
What pumps are required to reach region D Region D [10^-11 to 10^-15 Torr]?
Definition
Requires a combination of cryo and sublimation pumps in addition to other specialized pumps.
Term
How does a rough (rotary) pump work?
Definition
A vane sweeps out the volume as the pump rotates pushing the gas through an outlet and into oil. The gas from the chamber comes back into the pump at the inlet and it is swept away and so on.
Term
How does an oil diffusion pump work?
Definition
Molecules of a gas being pumped diffuse in to a jet of hot diffusion pump oil, which carries them along by viscous flow inside a condenser in which the vapor is gradually condensed into a liquid of low vapor pressure.
Term
How does a turbo molecular pump work?
Definition
A turbine like rotar rotates ata aspeed that exceeds the mean molecular speed of all ordinary components of air. The rotars smash into the molecules being pumped and remove them.
Term
How does an Ion pump work?
Definition
Ionization of atoms/molecules forcing them to a cathode. Ionized atoms/molecules smash into a titanium wall and imbed in it.
Term
How does a sublimation pump work?
Definition
Titanium is heated until it vaporizes. The Ti vapor pick up gas molecules/atoms. the Ti-gas vapor condenses on the container wall and traps the gas.
Term
How does a cryo pump work?
Definition
A large surface area chilled to liquid He temp (4.2K) adsorbs the gas molecules to be pumped.
Term
What are the gauges that measure pressure and what ranges do the cover?
Definition
1] Mercury manometer [1000 to 1 Torr]
2] Oil manometer [10 to 0.03 Torr]
3]Thermocouple Gauge [760 to 10^-3 Torr]
4] Pirani Gauge [10-10^-4 Torr]
5]Capacitance manometer [1000-10^-4 Torr]
6]McLeod Gauge [1-10^-5 Torr]
7] Ionization Gauge [10^-3 to 10^-12 Torr]
Term
How does a mercury manometer [1000 to 1 Torr] work?
Definition
Works on the principle of Boyle’s Law and compression of a known volume. Boyle’s Law: Volumelow x Pressurelow = Volumehigh x PressureHigh. High and low can be replaced with final and initial if need be.
Term
How does an oil manometer [10 to 0.03 Torr] work?
Definition
Works on the principle of Boyle’s Law and compression of a known volume. Boyle’s Law: Volumelow x Pressurelow = Volumehigh x PressureHigh. High and low can be replaced with final and initial if need be.
Term
How does a Thermocouple Gauge [760 to 10^-3 Torr] Work?
Definition
Measures the temperature of a filament as the thermal conductivity of a gas changes with pressure
Term
How does a Pirani Gauge [10 to 10^-4 Torr] work?
Definition
Measure the resistance of a filament as its temperature changes due to a change in the thermal conductivity of a gas with changing pressure.
Term
How does a Capacitence Manometer [1000-10^-4 Torr] work?
Definition
Changes in pressures cause deflections in a capacitor membrane. Pressure readings made based on change in capacitance.
Term
How does a McLeod Gauge [1-10^-5 Torr] work?
Definition
Works on the principle of Boyle’s Law and compression of a known volume. Boyle’s Law: Volumelow x Pressurelow = Volumehigh x PressureHigh. High and low can be replaced with final and initial if need be.
Term
How Does an Ionization Gauge [10^-3 to 10^-12 Torr] work?
Definition
Molecules and atoms are ionized. The ion current of the resulting ions is indicative of the pressure.
Term
What is conductivity with regard to pumping?
Definition
A given segment, i, of a pumping apparatus conducting the gas, may be said to have conductance Ci which is the flux, Q, in the gas through it divided by the pressure difference: Ci = Q/ (P1i – P2i)
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