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Isomerization of Carvone
Isomerization of Carvone
15
Organic Chemistry
Undergraduate 2
06/05/2019

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Term
what you will be transforming in this lab
Definition
transforming (R)-carvone to carvacrol
Term
the type of reaction you will be doing here
Definition
an acid-catalyzed isomerization reaction
Term
the acid that will be used in this experiment
Definition
sulfuric acid
Term
a hazard of sulfuric acid
Definition
severe burns
Term
How is the double extraction done?
Definition
by treating the layer containing the product with hexanes or petroleum ether twice
Term
Why a double extraction is used for this experiment
Definition
to remove all the product
Term
why the mixture containing the product is "washed" with water
Definition
to remove excess acid
Term
what sodium bicarbonate is used for in this experiment
Definition
to remove excess acid

the misture is washed with sodium bicarbonate to remove excess acid
Term
what brine is used for in this experiment
Definition
to dry the organic layer
Term
what anhydrous sodium sulfate is used for in this experiment
Definition
to dry the mixture
Term
what a rotary evaporator is used for in this experiment
Definition
to remove the organic solvent
Term
extract
Definition
taking something out of something else into something you want

you want to keep what you extract into
example: keep coffee, but not the grinds
Term
wash
Definition
rinse the desired layer with a solvent or solution to remove an impurity
Term
what to do when you're done with the experiment
Definition
1: get the mass of the product to get % yield
2: take an NMR of the compound to determine the identity
3: develop the mechanism
Term
where organic waste has to go
Definition
the organic waste container
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